The logical framework of the continuous Joule heating method. (IMAGE)
Caption
(a) The logical framework of the continuous Joule heating method. (b) Diagrammatic sketch of updated continuous FJH synthesis was designed for improving production efficiency, which was constructed by the integration of multiple reaction electrodes with respective independent power. A: a loading area or collecting area, B: a reaction area (magnified view for reactor), C: corresponding to respective independent power in the interior of the device, D: PLC platform, and E: a robotic arm. (c) Recorded voltage and current of FJH continued synthesis processes to prepare ternary metal material (including Cu, V, and Fe elements) for five batches (samples 1–5). (d) CAP degradation profiles of ternary metal material prepared by continuous FJH method. Degradation conditions: CCAP,0 = 60 mg·L−1, Cmaterial = 1000 mg·L−1, CPDS = 7 mmol·L−1, initial pH0 = 3.0 ± 0.2, temperature = 28 oC. The experiments were repeated twice. (e) TEM with an EDS pattern (different elements represent different colors) of ternary metal material prepared by continuous FJH method.
Credit
Xiangdong Zhu, Beibei Xiao, Fengbo Yu, Chao Jia, Liming Sun, Shicheng Zhang, Lianli Wang, Peixin Cui, Liang Wang, Xiaoguang Duan, Shaobin Wang, Yujun Wang
Usage Restrictions
Credit must be given to the creator. Only noncommercial uses of the work are permitted. No derivatives or adaptations of the work are permitted.
License
CC BY-NC-ND