Table 1. Optimization of electrogenerated acid-catalyzed glycosylation (IMAGE)

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Table 1. Optimization of electrogenerated acid-catalyzed glycosylation

Caption

Reaction conditions: a1a (0.2 mmol), 2a (0.24 mmol), platinum plate (1.0 cm × 2.0 cm) and carbon cloth (1.0 cm ×2.0 cm), solvent (5.0 mL), 25 oC, 10 mins, in an undivided cell. Yields and α/β ratios were determined by 1H NMR analysis of the crude mixtures with mesitylene as internal standard; bisolated yield in parenthesis; cwith platinum plate anode and carbon cloth cathode, 10 min.

Credit

Yaoyao Liu, Ting Chen, Jun-Jie Ying, Zhichao Zhang, Bo Duan, Pan Fang, Wei-Jun Kong

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